Standard Test Method for Analysis of Carbon and Low-Alloy Steel by Spark Atomic Emission Spectrometry – ASTM E Standard Number, ASTM E – Title, Standard Test Method for Analysis of Carbon and Low-Alloy Steel by Spark Atomic Emission. Designation: E − 15Standard Test Method for Contact ASTM Customer Standards volume information, refer to the standard’s Document Summary page.

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NOTE 9—The manner and frequency of positioning or checking the position of the exit slits will depend on factors such as: The reference materials and specimens should be of similar metallurgical condition and composition. xstm

ASTM E415 – 17

Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk of infringement of such rights, are entirely their own responsibility. Reagents and Materials 7. Summary of Test Method 4.

Last previous edition E — Originally published as E — Make the necessary corrections either by adjusting the controls on the readout or by applying arithmetic corrections. Cut a 13 to mm 1? Condition a fresh counter electrode with two to six excitations using the operating conditions in accordance with B Interferences are dependent upon instrument design, dispersion, spectrum line choices, and excitation conditions, and those listed require con?

If readings are not in conformance, repeat the standardization. It e4155 assumed that all who use this test method will be analysts capable of performing common laboratory procedures skillfully and safely. With that equipment, a smooth, white, texture burn without the characteristic dark ring indicates an improperly excited specimen. Its approximate range shall be from Once established, maintain the parameters consistently.


The potentials on the capacitors may be read directly, or axtm number of different readout systems may be employed which yield linear or logarithmic functions of the potentials and which may be displayed as relative numbers or as numbers calibrated directly in terms of percent. Enter your personal account email address to request a password reset: With a thoriated tungsten electrode, it has been reported that a hundred or more e4415 can usually be made before replacement.

It is designed for either chill-cast or rolled and forged specimens. Enter your account email address to request a password reset: Make certain that the specimens are homogeneous and free from voids and pits in the region ee415 be excited Note 5. No items in cart. NOTE 12—A high-purity argon atmosphere is required at the analytical gap. NOTE 14—With certain spectrometers, a properly excited specimen usually exhibits a dark ring around the pitted sparked area.

Center the analytical gap on the optical axes of the spectrometer.


Means of changing the? The discharge is terminated at a predetermined intensity time integral of a selected iron line, or at a predetermined time, and the relative radiant energies or concentrations of the analytical lines are recorded.

Using the averages of the data for each point, determine analytical curves as directed in Practices Zstm and E Calibration, Standardization, and Veri? Active view current version of standard. Use either a 3, 4, or 5-mm The specimen thickness should be between 10 and 38 mm. The number of acceptable excitations on an electrode varies from one instrument to another, aastm should be established in each laboratory. Your comments are invited either for revision of this standard or for additional standards asym should be addressed to ASTM Headquarters.


Current edition approved Nov. Better performance is expected when reference materials and specimens ast of similar metallurgical condition and composition.

Other internal standard and analytical lines, such as those listed in Table 2, may be used provided that it can be shown experimentally that equivalent precision and accuracy are obtained.

The specimen thickness can vary significantly according to the design of the spectrometer stand, but a thickness between 10 mm and 38 mm has been found to be most practical. NOTE 4—A black deposit builds up on the tip of the electrode, thus reducing the overall intensity of the spectral radiation. FORMAT Single User Subscription Site License Subscription BOOKS All Books PACKAGES All Astk EDITION to PUBLISHER.

In general this condition will not astk analytical performance for the?

It is designed for chill-cast, rolled, and e4115 specimens. Work Item s – proposed revisions of this standard. Automatic sequencing shall be provided to actuate the? Land Use and Development. Are you sure you want to empty the cart? Remember me for one month. For this purpose, veri?

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